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高灵敏度锥形光纤SERS探针及其在农残检测中的应用
High Sensitivity Tapered Fiber SERS Probe and Its Application on Pesticide Residues Detection

查看参考文献22篇

雷星 1   刘晔 1 *   黄竹林 2   姚波 1   毛庆和 1 *  
文摘 实验研究了激光诱导化学沉积法(LICDM)中诱导激光功率及诱导时间对锥形光纤表面增强拉曼散射(SERS)探针性能的影响。通过优化激光诱导功率为90 m W、诱导时间为50 min,制备出高灵敏度的锥形光纤SERS探针,结合便携式拉曼光谱仪实现了1.0×10~(-7)mol/L甲基对硫磷(MP)的检测;该方法制备的探针对MP的SERS光谱检测具有良好的重复性。这种高灵敏度、可重复性好的锥形光纤SERS探针在农残现场检测、定量分析等方面具有潜在的应用前景。
其他语种文摘 The influences of induced laser power and reaction time on the properties of tapered fiber surface enhanced Raman scattering (SERS) probes by the laser induced chemical deposition method (LICDM) are studied in experiments. Under an optimized experimental conditions as 90 mW induced laser power and 50 min reaction time, the prepared taper fiber SERS probes possess the highest sensitivity, when detecting a low concentration as 1.0 × 10~(- 7) mol/L of methyl parathion (MP) solution with a portable Raman spectrometer. Moreover, the prepared probes with LICDM show good repeatability for SERS detections, which may have potentials on rapid and field detection of pesticide residues.
来源 光学学报 ,2015,35(8):0806001-1-0806001-7 【核心库】
DOI 10.3788/AOS201535.0806001
关键词 光纤光学 ; 锥形光纤SERS探针 ; 激光诱导化学沉积法 ; 表面增强拉曼散射 ; 甲基对硫磷
地址

1. 中国科学院安徽光学精密机械研究所, 安徽省光子器件重点实验室, 安徽, 合肥, 230031  

2. 中国科学院固体物理研究所, 中国科学院材料物理重点实验室;;安徽省纳米材料和纳米技术实验室, 安徽, 合肥, 230031

语种 中文
文献类型 研究性论文
ISSN 0253-2239
学科 电子技术、通信技术
基金 国家自然科学基金 ;  国家973计划
文献收藏号 CSCD:5527777

参考文献 共 22 共2页

1.  Alak A. Surface-enhanced Raman spectrometry of organophosphorus chemical agents. Anal Chem,1987,59(17):L2149-L2153 被引 11    
2.  Kang T. Methyl parathion sensors based on gold nanoparticles and nafion film modified glassy carbon electrodes. Sensors and Actuators B,2010,145(1):104-109 被引 2    
3.  Zhou Y. Multifunctional TiO_2-coated Ag nanowire arrays as recyclable SERS substrates for the detection of organic pollutants. Eur J Inorg Chem,2012,2012(19):3176-3182 被引 3    
4.  Wang J. Synthesis of novel decorated one-dimensional gold nanoparticle and its application in ultrasensitive detection of insecticide. J Mater Chem,2010,20(25):5271-5279 被引 7    
5.  Lee D. Quantitative analysis of methyl parathion pesticides in a polydimethylsiloxane microfluidic channel using confocal surface-enhanced Raman spectroscopy. Appl Spec,2006,60(4):373-377 被引 9    
6.  Li J F. Shell-isolated nanoparticle-enhanced Raman spectroscopy. Nature,2010,464(7287):392-395 被引 245    
7.  Zhang L. Self-assembly Ag nanoparticle monolayer film as SERS substrate for pesticide detection. Applied Surface Science,2013,270:292-294 被引 5    
8.  Viets C. Comparison of fibre-optic SERS sensors with differently prepared tips. Sens Actuators B,1998,51(1/3):92-99 被引 11    
9.  Viets C. Fibre-optic SERS sensors with conically etched tips. J Mol Struct,2001,563:163-166 被引 9    
10.  Polwart E. Novel SERS-active optical fibers prepared by the immobilization of silver colloidal particles. Appl Spectrosc,2000,54(4):522-527 被引 11    
11.  徐蔚青. 银溶胶自组装表面增强光纤拉曼探针的研究. 光散射学报,2003,14(4):238-241 被引 1    
12.  Lucotti A. Use of a geometry optimized fiber-optic surface-enhanced Raman scattering sensor in trace detection. Appl Spectrosc,2007,61(3):260-268 被引 5    
13.  Lucotti A. Fiber-optic SERS sensor with optimized geometry. Sens Actuators B,2007,121(2):356-364 被引 10    
14.  Andrade G. Multilayer silver nanoparticles-modified optical fiber tip for high performance SERS remote sensing. Biosensors and Bioelectronics,2010,25(10):2270-2275 被引 1    
15.  贾少杰. 激光诱导沉积银膜制备光纤SERS传感器. 高等学化学学报,2006,27(3):523-526 被引 6    
16.  Li M S. Laser-Induced Silver Nanoparticles Deposited on Optical Fiber Core for Surface-Enhanced Raman Scattering. Chin Phys Lett,2010,27(4):044202 被引 4    
17.  Zheng X L. Photochemical modification of an optical fiber tip with a silver nanoparticle film: a SERS chemical sensor. Langmuir,2008,24(8):4394-4398 被引 10    
18.  Liu T. Surfactantless photochemical deposition of gold nanoparticles on an optical fiber core for surfaceenhanced Raman scattering. Langmuir,2011,27(8):4623-4626 被引 6    
19.  Thrall E S. R6G on graphene: High Raman detection sensitivity, yet decreased Raman cross-section. Nano Lett,2012,12(3):1571-1577 被引 7    
20.  Fan Q. Investigations of the fabrication and the surface-enhanced Raman scattering detection applications for tapered fiber probes prepared with the laser-induced chemical deposition method. Appl Opt,2013,52(25):6163-6169 被引 2    
引证文献 6

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