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Preparation of ZrN-Si_3N_4 composite powder with zircon and carbon black as raw materials

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文摘 ZrN-Si_3N_4 composite powder with low cost from zircon was prepared by carbothermal reduction-nitridation process. The influence of mass ratio of C to ZrSiO_4 (m(C)/m(ZrSiO_4)) and soaking time on phase composition and microstructure of the products was studied by means of XRD and SEM-EDS. The formation process of ZrN-Si_3N_4 composite powder was also analyzed in detail. The results show that with the increase of m(C)/m(ZrSiO_4) and soaking time, the formation of Si_3N_4 and ZrN can be promoted obviously. The ZrN-Si_3N_4 composite powder with size of 1-2 μm can be obtained at 1 773 K for 12 h when m(C)/m(ZrSiO_4) is 0.4.
来源 Transactions of Nonferrous Metals Society of China ,2009,19(5):1222-1226 【核心库】
DOI 10.1016/s1003-6326(08)60432-x
关键词 ZrN ; Si_3N_4 ; zircon ; carbothermal reduction
地址

School of Materials and Metallurgy, Northeastern University, Liaoning, Shenyang, 110004

语种 英文
文献类型 研究性论文
ISSN 1003-6326
学科 金属学与金属工艺
基金 国家自然科学基金委员会-上海宝钢集团公司“钢铁联合研究基金”
文献收藏号 CSCD:3712113

参考文献 共 15 共1页

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引证文献 2

1 Yu Renhong Thermodynamic Analysis and Preparation of Composites in Zr-Si-C-N-O System 稀有金属材料与工程,2014,43(2):301-305
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2 廖圣俊 高导热氮化硅陶瓷基板研究现状 材料导报,2020,34(11A):21105-21114
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