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偏压和氮分压对TiN膜层结构和膜/基体系性能的影响
Influence of Bias Voltage and N_2 Partial Pressure on Structure of TiN Film and Performance of Film/Substrate

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文摘 采用多弧离子镀工艺在钛合金或低碳钢基材上制备TiN薄膜,研究了不同偏压及不同氮分压下制备的薄膜相结构、残余应力、膜/基体系硬度、膜/基结合及其摩擦磨损行为.结果表明:偏压影响TiN晶粒的择优取向,偏压绝对值越大则薄膜内部的残余应力也越大;偏压过高或过低都会降低薄膜与基材之间的结合强度,从而影响其摩擦学性能.氮分压上升,TiN熔滴粒度变大,Ti_2N相减少,导致薄膜硬度提高;由过高或过低氮分压制备的膜/基体系在划痕试验中测得的临界载荷均较小;随着氮分压的增加,在试验范围内样品的摩擦因数下降但耐磨性并未获得预期的提高.
其他语种文摘 The TiN film was prepared by multi-arc ion plating process on titanium alloy substrate or carbon steel substrate with different bias voltage and different nitrogen partial pressure. The phase structure, residual stress inside film, hardness of film/substrate system, adhesive strength between film and substrate, and tribolocical behavior were studied. The test results show that the bias voltage affects phase structure and residual stress of film. The adhesive strength of film/substrate will decrease and the tribological performance will be affected consequently when bias voltage is excessive high or low. As N_2 partial pressure increases the particle size of Ti molten droplet becomes large, the amount of Ti_2N decreases, and the hardness of film heightens. The excess on highness or lowness of N_2 partial pressure can decrease critical load in scratching test. In the range of the tests, the friction coefficient of film/substrate system was decreased but wear resistance was not expectant improved with the increase of N_2 partial pressure.
来源 中国表面工程 ,2009,22(2):20-25 【扩展库】
关键词 微纳米材料 ; 摩擦磨损 ; 润滑 ; 自修复
地址

中国科学院,金属研究所, 辽宁, 沈阳, 110016

语种 中文
文献类型 研究性论文
ISSN 1007-9289
学科 金属学与金属工艺
基金 国家自然科学基金
文献收藏号 CSCD:3525477

参考文献 共 12 共1页

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引证文献 6

1 崔贯英 多弧离子镀(Ti, Al, Zr)N多元超硬梯度膜的制备及力学性能研究 真空科学与技术学报,2010,30(3):329-333
被引 6

2 吕会敏 (Ti, Al, Zr)N多元氮梯度硬质反应膜的组织结构和性能 材料研究学报,2011,25(1):89-94
被引 1

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